PREPARATION OF META-NITROBENZOYLHYDRAZONE FERROCENOYLACETONE AND SYNTHESIS ON ITS BASIS
##plugins.themes.bootstrap3.article.main##
Аннотация
β-diketone-ferrocenoylacetone was obtained by Claisen condensation. Meta-nitrobenzoylhydrazone of
ferrocenoylacetone (H2L) was synthesized by the interaction of meta-nitrobenzoic acid hydrazide with ferrocenoylacetone. On
its basis, complexes with copper(II) and nickel(II) ions were synthesized. The obtained compounds were characterized by the
methods of elemental analysis, IR-, 1H NMR andelectronic spectroscopy
##plugins.themes.bootstrap3.article.details##
Библиографические ссылки
L.V.Snegur, Yu.S.Nekrasov, N.S.Sergeeva, Zh.V.Zhilina, V.V.Gumenyuk, Z.A.Starikova, A.A.Simenel, N.B.Morozova,
I.K.Sviridova, V.N.Babin, “Ferrocenylalkylazoles: bioactivity, synthesis, structure”, Appl. Organomet. Chem., no. 22,
pp. 139-147, 2008.
L.V.Popova, V.N.Babin, Yu.A.Belousov, Yu.S.Nekrasov, A.E.Snegireva, N.P.Borodina, G.M.Shaposhnikova,
O.B.Bychenko, P.M.Raevskii, N.B.Morozova, A.I.Iiyina, K.G.Shitkov, “Antitumor effects of binuclear ferrocene
derivatives”, Appl. Organometal. Chem., no. 7, pp. 85-94, 1993. https://doi.org/10.1002/aoc.590070203
N.J.Forrow, N.C.Foulds, J.E.Frew, J.T.Law, “Synthesis, Characterization, and Evaluation of Ferrocene−Theophylline
Conjugates for Use in Electrochemical Enzyme Immunoassay”, Bioconjugate Chem., no. 15, pp. 137-144, 2004.
L.V.Snegur, V.N.Babin, A.A.Simenel, YU.S.Nekrasov, L.A.Ostrovskaya, N.S.Sergeeva, “Protivoopuholevaya aktivnost'
soedineniy ferrocena (obzor)” [Antitumor activity of ferrocene compounds (review)], Izvestiya AH. Ser.him., pp. 2113-2124,
(in Russian).
B.B.Umarov, Z.A.Sulaymonova, D.M.Tillaeva, “Sintez ligandov na osnove proizvodny'h ferrocena s gidrazidami mono- i
dikarbonovy'h kislot” [Synthesis of ligands or the basis of ferrocene derivatives with hydrazides of mono-, dicarboxylic acids],
Universum: Himiya i biologiya: e`lektron.nauchn. jurn., no. 3(69), pp. 19-22, 2020. (in Russian). URL:
http://7universum.com/ru/nature/archive/item/8966
B.B.Umarov, Z.A.Sulaymonova, D.M.Tillaeva, “Kompleksny'e soedineniya perehodny'h metallov na osnove kondensacii
proizvodny'h ferrocena s gidrazidami karbonovy'h kislot” [Complex compounds of transition metals or bases of condensation
of ferrocene derivatives as carboxylic acid hydrazides], Nauchny'y vestnik Namanganskogo gosudarstvennogo universiteta,
no. 9, pp. 58-63, 2020. (in Russian).
B.B.Umarov, Z.A.Sulaymonova, M.K.Achy'lova, “Sintez kompleksov na osnove monokarbonil'ny'h proizvodny'h ferrocena
s gidrazidami karbonovy'h kislot” [Synthesis of complexes or the basis of monocarbonyl derivatives of ferrocene with
carboxylic acid hydrazides], Universum: Himiya i biologiya: e`lektron. Nauch. Jurn., no. 1(79), pp. 85-91, 2021. (in Russian).
URL: (http://7universum.com/ru/nature/archive/item/category/179/). (in Russian).
S.I.Yakimovich, V.N.Nikolaev, E`.Yu.Kucenko, “Tautomeriya v ryadu acilgidrazonovformilpinakolina” [Tautomerism in the
series of acylhydrazones of formylpinacoline], Jurn. Org. Himii, vol. 27, no. 5, pp. 959-965, 1991. (in Russian).
O.Ya.Neyland, Ya.P.Strady'n', E`.A.Silin'sh i dr., Stroenie i tautomerny'e prevrasch'eniya vdikarbonil'ny'h soedineniy
[Structure and tautomeric transformations of dicarbonyl compounds]. Riga: Zinatne, 1977. (in Russian).
V.A.Kogan, A.N.Morozov, V.V.Lukov, “Fiziko-himicheskoe issledovanie kompleksov na osnove aroilgidrazonovferrocena”
[Physico-chemical study of complexes based on ferrocene aroylhydrazones], Jurn. neorg. Himii, vol. 33, no. 1, pp. 133-138,
(in Russian).
E.R.Lippincott, R.D.Nelson, “J. Amer. Chem.” Soc. -77, N 19. -1995, 4990 p.
L.Bellami, Infrakrasny'e spektry' slojny'h molekul [Infrared spectra of complex molecules]. Moskva: IL,1963. (in Russian).
G.B.Zaslonskaya, B.M.Yavorskiy, N.S.Kochetkova, N.P.Gambaryan, Dokl. AN SSSR, no. 3, 1957, 433 p. (in Russian).
H.Imai, Y.Yaehashi, “Nippon Karaku Zasshi” no. 5, 1970, 452 p.
H.Hennig, O.Gurtler, “J. Organomet.Chem” no. 2, 1968, 307 p.
W.Bell, J.A.Crayston, C.Glidewell et al., “J.Organomet. Chem”, 1992, 115 p