SYNTHESIS AND STUDY OF MONOACETYLFERROCENE BENZOYLHYDRAZONE AND ITS COMPLEX WITH CHROMIUM(III) ION
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Аннотация
Hydrazone was synthesized by the interaction of benzoic acid hydrazide with monoacetylferrocene. Based on them, a complex compound with a chromium(III) ion was obtained. The elemental composition was determined by scanning electron microscopy with energy dispersive analysis. Based on the SEM and EDA data, it can be concluded that the complex formation of a metal
ion with an organic ligand leads to a change in their microstructure; in particular, numerous peaks of elements were recorded, which was confirmed by EDA. The IR spectrum was taken to elucidate the nature of the binding of the ligand co-ordination center to the central atom of the metal, the complex
compound synthesized by us.
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Библиографические ссылки
Ileaney E.K., Logan S.R. Photochemical reactions of acetylferrocene // Inorganica Chimica
Acta. - 1977. - V. 22. - P. 65-78.
Py F.F., Che D., Li G., Yao X.L., Zou D.P. Photo-induced ligand exchange reactions of ferrocenylacetylacetone in the presence of pyridine or 4,4-dipyridyl: Crystal and molecular structure of trans-bis(ferrocenylacetylacetonato) dipyridineiron(II) // J. Organomet. Chem. - 1998. - V. 568. -
P. l 65-169.